Motion For Bond Reduction With Sodium Borohydride
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How to fill out Louisiana Motion For Bond Reduction And Order?
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FAQ
Using method of the present invention is: after the reduction reaction of sodium borohydride terminates, under normal temperature, stir, this cancellation system is slowly added drop-wise in reaction mixture until the pH=7 of reaction solution, after being spin-dried for reaction solvent (such as methyl alcohol, ...
Sodium borohydride is a relatively selective reducing agent. Ethanolic solutions of sodium borohydride reduce aldehydes and ketones in the presence of epoxides, esters, lactones, acids, nitriles, or nitro groups. Reduction of aldehydes is straightforward.
The Bayer Process is a one-pot synthesis combining borax, metallic sodium, and hydrogen in the presence of silica to produce sodium borohydride. Na2B4O7 + 16 Na + 8 H2 + 7 SiO2 ? 4 NaBH4 + 7 Na2SiO3 (2a) 4 Page 7 DOE Cooperative Agreement DE-FC36-04GO14008 The reaction takes place at about 700 °C.
NaBH4 is usually used in hydroxylic solvents such as MeOH, EtOH, and H2O. Sometimes THF is used as a solvent, either alone or as a solvent mixture (ex. THF/MeOH or THF/EtOH). In MeOH and EtOH, NaBH4 decomposes over time to give the respective borates.
Sodium borohydride (NaBH4) was synthesized by reacting sodium metaborate (NaBO2) with magnesium hydride (MgH2) or magnesium silicide (Mg2Si) by annealing at 350-750° under a high H2 pressure of 0.1-7 MPa for 2-4 h.