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CHEM 2423 Recrystallization of Benzoic Acid Dr. Pahlavan EXPERIMENT 4 Purification Recrystallization of Benzoic acid Purpose: a) To purify samples of organic compounds that are solids at room temperature.

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Purpose/Introduction The process of recrystallization is an important method of purifying a solid organic substance using a hot solution as a solvent. This method will allow the separation of impurities.

When recrystallized using just water as the solvent the benzoic acid appeared as a white, powdery solid weighing . 87g. The percent recovery was 79%. The melting point of the crude benzoic acid was 118-122 C, while the melting point of the recrystallized benzoic acid was 121-127 C.

In a traditional organic laboratory experiment, insoluble impurities are removed through the recrystallization of benzoic acid utilizing water as the recrystallization solvent.

When recrystallized using just water as the solvent the benzoic acid appeared as a white, powdery solid weighing . 87g. The percent recovery was 79%. The melting point of the crude benzoic acid was 118-122 C, while the melting point of the recrystallized benzoic acid was 121-127 C.

Discussion and Conclusion: The percentage yield for benzoic acid and acetanilide acid being high indicated the initial sample had a low concentration of impurities. With the melting point being in a specific range it is concluded that benzoic acid and acetanilide is a pure substance after recrystallization was done.

AIM: To prepare crystals of pure benzoic acid from an impure sample. Theory: Benzoic acid is a crystalline solid has high solubility in hot water.an impure sample of benzoic acid is dissolved in hot water and then filtered to remove insoluble impurities.

Recrystallization is a method of purifying a compound by removing any impurities that might be mixed with it. It works best when the compound is very soluble in a hot solvent, but very insoluble in the cold version of the same solvent. The compound must be a solid at room temperature.

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Form Packages
Adoption
Bankruptcy
Contractors
Divorce
Home Sales
Employment
Identity Theft
Incorporation
Landlord Tenant
Living Trust
Name Change
Personal Planning
Small Business
Wills & Estates
Packages A-Z
Form Categories
Affidavits
Bankruptcy
Bill of Sale
Corporate - LLC
Divorce
Employment
Identity Theft
Internet Technology
Landlord Tenant
Living Wills
Name Change
Power of Attorney
Real Estate
Small Estates
Wills
All Forms
Forms A-Z
Form Library
Customer Service
Terms of Service
Privacy Notice
Legal Hub
Content Takedown Policy
Bug Bounty Program
About Us
Blog
Affiliates
Contact Us
Delete My Account
Site Map
Industries
Forms in Spanish
Localized Forms
State-specific Forms
Forms Kit
Legal Guides
Real Estate Handbook
All Guides
Prepared for You
Notarize
Incorporation services
Our Customers
For Consumers
For Small Business
For Attorneys
Our Sites
US Legal Forms
USLegal
FormsPass
pdfFiller
signNow
airSlate WorkFlow
DocHub
Instapage
Social Media
Call us now toll free:
+1 833 426 79 33
As seen in:
  • USA Today logo picture
  • CBC News logo picture
  • LA Times logo picture
  • The Washington Post logo picture
  • AP logo picture
  • Forbes logo picture
© Copyright 1997-2025
airSlate Legal Forms, Inc.
3720 Flowood Dr, Flowood, Mississippi 39232